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ASTM C791 : 12

Standard Test Methods for Chemical, Mass Spectrometric, and Spectrochemical Analysis of Nuclear-Grade Boron Carbide

Standard Details

1.1 These test methods cover procedures for the chemical, mass spectrometric, and spectrochemical analysis of nuclear-grade boron carbide powder and pellets to determine compliance with specifications.

1.2 The analytical procedures appear in the following order:

Sections
Total Carbon by Combustion in an Inductive Furnace and Infrared Measurement7-16
Total Boron by Titrimetry and ICP OES17-27
Isotopic Composition by Mass Spectrometry28-32
Pyrohydrolysis33-40
Chloride by Constant-Current Coulometry41-49
Chloride and Fluoride by Ion-Selective Electrode50-58
Water by Constant-Voltage Coulometry and Weight Loss on Drying59-62
Metallic Impurities63 and 64
Soluble Boron by Titrimetry and ICP OES65-79
Free Carbon by a Coulometric Method80-89

General Information

Status : Historical
Standard Type: Main
Document No: ASTM C791 : 12
Document Year: 2012
Pages: 25
  • Section Volume:
  • 12.01 Volume 12.01 Nuclear Energy (I)
  • ICS:
  • 27.120.30 Fissile materials and nuclear fuel technology

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