ASTM D5335 : 99

1.1 This test method covers the laboratory determination of the linear (one-dimensional) coefficient of thermal expansion of rock using bonded electric resistance strain gages.

1.2 This test method is applicable for unconfined pressure conditions over the temperature range from 68 to 500°F (20 to 260°C).

Note 1-Unconfined tests performed at elevated temperatures may alter the mineralogy or grain structure of the test specimen. This alteration may change the physical and thermal properties of the test specimen. Note 2-The strain gages are mounted with epoxy. Most commercially available high temperature epoxies require elevated temperature curing. The elevated temperature required for this curing may alter the physical and thermal properties of the test specimen. Epoxy should be selected based upon the maximum expected test temperature. Room temperature curing epoxy should be used whenever possible.

1.3 The test specimens may be either saturated or dry. If saturated specimens are used, then the test temperature must be at least 5°C less than the boiling point of the saturating fluid in order to minimize vaporization of the fluid.

Note 3-When testing a saturated specimen, the moisture content of the specimen may change unless special precautions are taken to encapsulate the test specimen. Refer to 7.4.

1.4 For satisfactory results in conformance with this test method, the principles governing the size, construction, and use of the apparatus described in this test method should be followed. If the results are to be reported as having been obtained by this test method, then all pertinent requirements prescribed in this test method shall be met.

1.5 It is not practicable in a test method of this type to aim to establish details of construction and procedure to cover all contingencies that might offer difficulties to a person without technical knowledge concerning the theory of heat flow, temperature measurement, and general testing practices. Standardization of this test method does not reduce the need for such technical knowledge. It is recognized also that it would be unwise, because of the standardization of this test method, to resist in any way the further development of improved or new methods or procedures by research workers.

1.6 The values stated in inch-pound units are to be regarded as the standard. The SI units given in parentheses are for information only.

1.7 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.