ASTM E3203 : 19a

Standard Test Method for Determination of Lead in Dried Paint, Soil, and Wipe Samples by Inductively Coupled Plasma-Optical Emission Spectroscopy (ICP-OES)

Standard Details

1.1 This test method specifies a procedure for analysis of dried paint, soil, and dust wipe samples collected in and around buildings and related structures for lead content using inductively coupled plasma-optical emission spectroscopy (ICP-OES).

1.2 This test method should be used by analysts experienced in the use of ICP-OES, the interpretation of spectral and matrix interferences, and procedures for their correction. For determination of lead (Pb) and other metals in air by ICP-OES, see Test Method D7035.

1.3 This test method cites specific methods for preparing test solutions of dried paint, soil, and wipe samples for analysis.

1.4 It is the user’s responsibility to ensure the validity of this test method for sampling materials of untested matrices.

1.5 No detailed operating instructions are provided because of differences among various makes and models of suitable ICP-OES instruments. Instead, the analyst shall follow the instructions provided by the manufacturer of the particular instrument. This test method does not address comparative accuracy of different devices or the precision between instruments of the same make and model.

1.6 This test method contains notes that are explanatory and are not part of the mandatory requirements of this test method.

1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.7.1 Exception—The inch-pound and SI units shown for wipe sampling data are to be individually regarded as standard for wipe sampling data.

1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International StandardDetails, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.