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Plastics — Determination of dynamic mechanical properties — Part 10: Complex shear viscosity using a parallel-plate oscillatory rheometer
NOTE 1 The angular-frequency measurement range is limited by the specification of the measuring instrument and also by the response of the specimen. When testing using angular frequencies lower than 0,1 rad·s?1, the test time can increase significantly as the time taken to obtain a single measurement is proportional to the reciprocal of the angular frequency. Consequently, when testing at low angular frequencies, degradation or polymerization of the specimen is more likely to occur and have an effect on the results. At high angular frequencies, the specimen can distort or fracture at the edge, consequently invalidating the test results.
NOTE 2 The range of complex shear viscosity values that can be measured is dependent on the specimen dimensions and also the specification of the measuring instrument. For a specimen of given dimensions, the upper limit of the range is limited by the machine's torque capacity, angular-displacement resolution, and compliance. However, correction can be made for compliance effects.
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