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ISO 1693:1976

Cryolite, natural and artificial — Determination of fluorine content — Modified Willard-Winter method

Standard Details

Specifies the determination for natural and synthetic materials having a molar ratio sodium fluoride/aluminium trifluoride between 3 and 1,7 approximately. The principle consists in fusion of a test portion with sodium carbonate, separation of fluorine by distillation with sulphuric acid or perchloric acid. Titration with thorium nitrate solution in presence of sodium alizarinsulphonate/methylene blue as indicator. Alternatively, the thorium nitrate titration may be made using only sodium alizarinsulphonate, the end-point being*spectrophotometrically determined at 525 nm.

General Information

Status : Published
Standard Type: Main
Document No: ISO 1693:1976
Document Year: 1976
Pages: 6
Edition: 1
  • Section Volume:
  • ISO/TC 226. Materials for the production of primary aluminium

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ISO 1693:1976
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